By Ronald S. Bauer (Eds.)
Content material: The photoinitiated cationic polymerization of epoxy resins / J.V. Crivello and J.H.W. Lam -- Photosensitized epoxides as a foundation for light-curable coatings / William R. Watt -- Quaternary phosphonium compound latent accelerators for anhydride-cured epoxy resins / James D.B. Smith -- improvement of epoxy resin-based binders for electrodeposition coatings with excessive corrosion resistance / W. Raudenbusch -- Water-borne coatings ready from excessive molecular weight epoxy resins / Edward G. Bozzi and Camilla Y. Zendig -- Aqueous epoxy resins for electric bolstered plastics / Terry L. Anderson, James H. Melloan, Kathleen L. Powell, Roland R. McClain, J. Brandon Simons, Robin L. Conway, and David A. Shimp -- Epoxide identical weight decision through carbon-13 nuclear magnetic resonance / W.B. Moniz and C.F. Poranski, Jr. -- An instrumental technique for measuring the sterilization resistance (blushing) of can coatings / W. Raudenbusch, H.C.J. Venselaar, and D.M. Paul -- Phenalkamines, a brand new type of epoxy curing brokers / Robert A. Gardiner and Anthony P. Manzara -- The impression of alkyl substituents at the houses of cured hydantoin epoxy resins / E.H. Catsiff, R.E. Coulehan, J.F. Diprima, D.A. Gordon, and R. Seltzer -- influence of cross-link density distribution at the engineering habit of epoxies / S.C. Misra, J.A. Manson, and L.H. Sperling -- community morphology and the mechanical habit of epoxies / S.C. Misra, J.A. Manson, and L.H. Sperling -- Creep habit of amine-cured epoxy networks : impact of stoichiometry / S.L. Kim, J.A. Manson, and S.C. Misra -- Self-cross-linkable polyepoxides / Yoshio Tanaka -- a few stories at the guidance of glycidyl 2-ethylhexanoate / D.A. Cornforth, B.G. Cowburn, K.M. Smith, C.W. Stephens, and C.G. Tilley -- Reactions in a standard epoxy-aliphatic diamine procedure / John J. King and James P. Bell -- Epoxy resins containing a selected vulnerability / James R. Griffith
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Ch003 MTBP-DMP BTPPC CH C 3 C H C H 6 5 2 C H 4 9 H C H 4 9 C C H 4 9 H 6 5 °6 5 0,Η 4 9 0,Η 4 9 MTPP-DMP 0,Η 4 9 CH 3 C 6 5 H C 6 5 H C 6 5 TPEPI C H C 6 5 H C 6 5 H C 6 5 TBPC Λ 2 5 Λ H 6 5 Λ 4 9 3 3 2 "CI "ci fl H 0 P(OCH ) H "i 3 2 Gel Time Data. I n i t i a l l y , gel times were recorded on 10 g samples of resin i n 2 i n . diameter aluminum dishes over the temperature range 135°C to 170°C Later, to give improved accuracy, the gel time measurements were made in 19 χ 150 mm test tubes in a constant temperature silicone o i l bath using a Sunshine Gel Meter.
S t i r r i n g at 0°C was continued f o r 10-15 minutes, then 15 m l . o f 65% aqueous hexafluorophosphoric a c i d was s l o w l y added, keeping the temperature of the r e a c t i o n mixture below 8°C. ( C a u t i o n : HPF a t t a c k s g l a s s . A l l p l a s t i c containers and labware should be used f o r handling and t r a n s f e r r i n g t h i s a c i d . ) S t i r r i n g and c o o l i n g were continued f o r 10-15 minutes a f t e r a l l the HPF had been added. The p r e c i p i t a t e d product was recovered by f i l t r a t i o n , washed w i t h c o l d water u n t i l free o f c h l o r i n e (AgN0 t e s t ) and a i r d r i e d on the f i l t e r .
Kester, D. E. Organic Coatings and Plastics Preprints, 1977, Am. Chem. Soc. 37, (2), 67-72 12. ; Dreyfuss, P. Polymer, 1965, 6, 93 13. ; Dreyfuss, P. J . Polymer S c i . , 1966, A-1, 4 2179-2200 14. Licari, J . ; Crepeau, P. C. ), September 7, 1965 15. Fischer, E. US 3,236,784 (Farbwerke Hoechst AG), February 22, 1966 16. Schlesinger, S. I . , Polymer Sci. and Eng. 1974, 14 (7),513-515 17. Schlesinger, S. I . , Photographic Sci. and Eng. ch002 44 EPOXY RESIN CHEMISTRY 18. Schlesinger, S. ), January 2, 1973 19.